Effect of Synthesis Temperature on the Growth of Carbon-based Materials from Waste Engine Oil Precursor

Authors

  • Suhufa Alfarisa Department of Physics, Universitas PGRI Palembang, Indonesia http://orcid.org/0000-0002-1142-4824
  • Suriani Abu Bakar Department of Physics, Faculty of Science and Mathematics Universiti Pendidikan Sultan Idris, Perak 35900 Malaysia

DOI:

https://doi.org/10.31851/jupiter.v1i1.3122

Keywords:

waste engine oil, carbon-based material, thermal chemical vapor deposition

Abstract

Different stuctures of carbon material were succesfully synthesized from waste engine oil (WEO) as carbon source using double-stage thermal chemical vapor deposition method. In this work, 5.33 wt% ferrocene was used as catalyst, precursor temperature at 450°C and the synthesis temperatures were varied from 600-1000°C with 100°C increament. The prepared samples were characterized using field emission scanning electron microscopy and micro-Raman spectroscopy. Below 700°C, amorphous structure of carbon was formed. Well growth carbon spheres were produced at 800°C while at 900°C, bigger diameter and lower crystallinity of carbon spheres were resulted. At very high temperature, 1000°C, a highly defective structure of carbon was produced. These results show that the structure of carbon materials from WEO precursor was highly affected by synthesis temperature changes

References

Ajayan, P. M. and O. Z. Zhou (2001). Applications of carbon nanotubes. Carbon Nanotubes, Springer: 391-425.

Alfarisa, S., R. N. Safitri, et al. (2016). "Effect of Catalyst Concentrations on the Growth of Carbon Nanotubes from Waste Engine Oil."

Alfarisa, S. and A. B. Suriani (2016). "Pemanfaatan Minyak Pelumas Bekas untuk Fabrikasi Bola Karbon Mikro menggunakan Metode Deposisi Uap Kimia Termal." Sainmatika: Jurnal Ilmiah Matematika dan Ilmu Pengetahuan Alam 13(1).

Asli, N. A., M. S. Shamsudin, et al. "Field electron emission properties of vertically aligned carbon nanotubes deposited on a nanostructured porous silicon template: The hidden role of the hydrocarbon/catalyst ratio." Microelectronic Engineering 108(0): 86-92.

Cheng, H. M., F. Li, et al. (1998). "Large-scale and low-cost synthesis of single-walled carbon nanotubes by the catalytic pyrolysis of hydrocarbons." Applied Physics Letters 72(25): 3282-3284.

Donev, L. A. K. (2009). Carbon nanotube transistors: Capacitance measurements, localized damage, and use as gold scaffolding, Cornell University.

Lou, Z., C. Chen, et al. (2006). "Large-scale synthesis of carbon spheres by reduction of supercritical CO< sub> 2 with metallic calcium." Chemical physics letters 421(4): 584-588.

Nowack, B., R. M. David, et al. (2013). "Potential release scenarios for carbon nanotubes used in composites." Environment international 59: 1-11.

Poudel, P. and Q. Qiao "Carbon nanostructure counter electrodes for low cost and stable dye-sensitized solar cells." Nano Energy(0).

Shanov, V., W. Cho, et al. (2013). "CVD growth, characterization and applications of carbon nanostructured materials." Surface and Coatings Technology 230(0): 77-86.

Suriani, A. B., S. Alfarisa, et al. (2015). "Quasi-aligned Carbon Nanotubes Synthesised from Waste Engine Oil." Materials Letters 139: 220-223.

Suriani, A. B., A. R. Dalila, et al. (2013). "Vertically aligned carbon nanotubes synthesized from waste chicken fat." Materials Letters 101(0): 61-64.

Suriani, A. B., R. Md Nor, et al. (2010). "Vertically aligned carbon nanotubes synthesized from waste cooking palm oil." Journal of the Ceramic Society of Japan 118(1382): 963-968.

Wilgosz, K., X. Chen, et al. (2012). "Template method synthesis of mesoporous carbon spheres and its applications as supercapacitors." Nanoscale research letters 7(1): 1-5.

Zobir, S. A. M., S. Abdullah, et al. "Synthesis of carbon nano- and microspheres using palm olein as the carbon source." Materials Letters 78(0): 205-208.

Downloads

Published

2019-08-04